HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13787828, compound → HCID 12929196, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13787828 | HCID 13787828 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 12929196 | HCID 12929196 | — |
Reaction Steps
Following the procedure set forth in Example 1, 43 g. of 1,5-dimethyl-4-n-propyl-4-(3-methoxyphenyl)piperidine was reacted with 276 g. of mercuric acetate in 717 ml. of five percent aqueous acetic acid to provide, after purification by distillation, 30.2 g. of 1,5-dimethyl-4-n-propyl-4-(3-methoxyphenyl)-1,4,5,6-tetrahydropyridine. B.P. 126°-138° C. at 0.15 torr.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04228288 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-986ee712030a46f6bf860f427e3e9e3c |
| Source note | uspto-grants-1980_10 |