HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl bromide → HCID 70585053, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 57293339 | HCID 57293339 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 70585053 | HCID 70585053 | — |
Reaction Steps
A mixture of 3-methoxy-14β-hydroxy-6-oxamorphinan (X) (0.005 m), allyl bromide (0.006 m) and potassium carbonate (2 g) in 20 ml acetonitrile is heated at reflux for 18 hours. The mixture is filtered and the filtrate concentrated. The residue is treated with water and extracted with ethyl acetate. The extracts are dried (Na2SO4) and concentrated to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04228285 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-79fcdc5b632a445f831f8d9d9abe0ef4 |
| Source note | uspto-grants-1980_10 |