反应详情

Reaction of 2-chloromethylpyrimidine with ethylenediamine by the procedure of Example 34 and reaction of the resulting N-(2-pyrimidylmethyl)ethylenediamine with methyl isothiocyanate by the procedure of Example 3(b) gives, after concentrating and chromatographing, N-methyl-N'-[2-(2-pyrimidylmethylamino)ethyl]-thiourea. This thiorea is reacted with lead cyanamide by the procedure of Example 3(b) to give the title compound.

1. customgives
2. concentrationafter concentrating
3. customThis thiorea is reacted with lead cyanamide by the procedure of Example 3(b)