HRID903830

反应详情

EQUATION

反应方程式

HRID 903830 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a solution of (-)-α-amino-3-(chloromethyl)-4-hydroxybenzeneacetic acid hydrochloride (1 g, 0.004 mole) in 20 ml of water is added carbonodithioic acid, O-ethyl ester, potassium salt (1.26 g, 0.08 mole). Within a few minutes a precipitate begins to form. The mixture is stirred at room temperature for 3 hours. The solid precipitate is filtered, washed with water and dried to give 58.3% of the title compound.

WORKUP

后处理

  1. waitWithin a few minutes a precipitate begins
  2. customto form
  3. filtrationThe solid precipitate is filtered
  4. washwashed with water
  5. customdried