HuagongsheHuagongshe Chemistry Print Report · For research reference only
alpha-Amino-4-hydroxy-3-[(methylthio)methyl]benzeneacetic acid → (-)-alpha-Amino-4-hydroxy-3-[(methylsulfinyl)methyl]benzeneacetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | alpha-Amino-4-hydroxy-3-[(methylthio)methyl]benzeneacetic acid | HCID 23329760 | — |
| Reactant | Sodium periodate | HCID 23667635 | — |
| Product | (-)-alpha-Amino-4-hydroxy-3-[(methylsulfinyl)methyl]benzeneacetic acid | HCID 23329781 | — |
Reaction Steps
To an aqueous solution (500 ml) of α-amino-4-hydroxy-3-[(methylthio)methyl]benzeneacetic acid (1 mole) is added sodium metaperiodate (1 mole). The mixture is stirred at room temperature for 5 hours, it is filtered and the filtrate is lyophilyzed to give a quantitative yield of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04229363 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-e867d02bbde24d569052386c0cf34be9 |
| Source note | uspto-grants-1980_10 |