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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 903864Generated: October 25, 2026

Methyl formate → N-formyl-4-(3-azidopropyl)-piperidine

https://huagongshe.com/reaction/903864

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl formateHCID 7865—
Reactant4-(3'-Azidopropyl)-piperidineHCID 13503220—
ProductN-formyl-4-(3-azidopropyl)-piperidineHCID 13503223—

Reaction Steps

A solution of 4-(3'-azidopropyl)-piperidine (1.5 g) in methyl formate (5 ml) was refluxed for 1 hour. Evaporation to dryness gave the desired compound as an oil. The IR-spectrum (CHCl3) showed strong bands at 2100, 1660, 1440 and 1270 cm-1.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04229443
Source datasetuspto-grants-1980_10
ORD IDord-8891c984c82044f09907d7e03b12e8ed
Source noteuspto-grants-1980_10