Ethanol → HCID 20528725, compound

HRID 903868Notes

Reaction equation

HRID 903868 reaction equation
Cl[C:2]([CH:4]1[CH2:11][CH:10]2[CH2:12][CH:6]([C:7](=[O:14])[NH:8][C:9]2=[O:13])[CH2:5]1)=[O:3].[CH2:15]([OH:17])[CH3:16]>>[C:2]([CH:4]1[CH2:11][CH:10]2[CH2:12][CH:6]([C:7](=[O:14])[NH:8][C:9]2=[O:13])[CH2:5]1)([O:17][CH2:15][CH3:16])=[O:3]

Participants

3

Reactant 2

HCID 702EthanolHCID 20528705HCID 20528705, compound

Product 1

HCID 20528725HCID 20528725, compound

Procedure

A mixture of 7-chlorocarbonyl-3-azabicyclo[3.3.1]-nonane-2,4-dione (2 g) and absolute ethanol (25 ml) was left overnight at room temperature and evaporated to leave the desired compound which was used in the next step without purification.

Workup

  1. customevaporated

Sources & evidence

ORD record
ord-489949cb585e4b2bba18fa4b8a1a3d69
Source dataset
uspto-grants-1980_10
Patent number
US04229443

Reaction notes

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