HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Butanol → HCID 178492027, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Butanol | HCID 263 | — |
| Reactant | Diisopropyl Ether | HCID 7914 | — |
| Reactant | Formamidine acetate | HCID 160693 | — |
| Reactant | 4-Methoxyphenylthiosemicarbazide | HCID 2826172 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178492027 | HCID 178492027 | 73% |
Reaction Steps
A mixture of 10 parts of 2-(4-methoxyphenyl)-hydrazinecarbothioamide, 10.6 parts of methanimidamide acetate and 80 parts of 1-butanol is stirred and refluxed for 1 hour. After cooling, water and 2,2'-oxybispropane are added, whereupon the product is precipitated. It is filtered off and dried, yielding 7.6 parts (73%) of 1-(4-methoxyphenyl)-1H-1,2,4-triazole-3-thiol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04229460 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-b88711fa01de4b2195d93bc9f17e8188 |
| Source note | uspto-grants-1980_10 |