化工社化工社 化学情報印刷レポート · 研究参考用
4-(Octyloxy)benzoic acid → 4-Octyloxy-3-bromobenzoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-(Octyloxy)benzoic acid | HCID 17231 | — |
| 反応物 | Bromine | HCID 24408 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 4-Octyloxy-3-bromobenzoic acid | HCID 23333447 | — |
反応手順
37.5 g (0.15 mole) of p-octyloxy benzoic acid are put in suspension in 108 ml of deionized water. The temperature of the reaction medium is brought to between 50° C. and 55° C. and 8.7 ml (0.17 mole) of bromine are added at this temperature over a period of 7 hours 30 minutes.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04230596 |
| 出典データセット | uspto-grants-1980_10 |
| ORD ID | ord-6bc3d61f74cc46fc879b3a8c9515d2cf |
| 出典メモ | uspto-grants-1980_10 |