HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → HCID 12506912, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | 2-Methylphenyl propanoate | HCID 221436 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 12506912 | HCID 12506912 | 65% |
Reaction Steps
To a solution of 0.1 mol of o-cresol propionate in 150 cc of CCl4 are added, with ultraviolet irradiation, in small fractions, and in proportion with the decoloration, 0.22 mol of bromine in 30 cc of CCl4, the solvent is removed and the residue is distilled under reduced pressure. The 1-propionoxy-2-bromomethylbenzene is obtained:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04230624 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-996d0a3ee36d4db295a568126e37bb6d |
| Source note | uspto-grants-1980_10 |