Hydrazinecarboxaldehyde → HCID 23333677, compound

HRID 904124Notes

Reaction equation

HRID 904124 reaction equation
[C:1]([CH:9]([CH:14]([CH3:16])[CH3:15])[CH2:10][C:11](O)=O)(=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH:17]([NH:19][NH2:20])=O.C(C(C)C(C)C(O)=O)(=O)C1C=CC=CC=1.C([NH:39][NH2:40])(=O)C>>[CH:14]([C:9]1[C:1]([C:2]2[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=2)=[N:20][N:19]2[CH:17]=[N:39][N:40]=[C:11]2[CH:10]=1)([CH3:16])[CH3:15]

Participants

5

Reactant 4

HCID 12229HydrazinecarboxaldehydeHCID 14039AcetohydrazideHCID 12240573HCID 12240573, compoundHCID 23333667HCID 23333667, compound

Product 1

HCID 23333677HCID 23333677, compound

Procedure

The procedure of Example 4 is repeated substituting equimolecular amounts of 3-benzoyl-3-isopropyl-propionic acid and N-formylhydrazine for the 3-benzoyl-2,3-dimethyl-propionic acid and N-acetylhydrazine employed in that example. There is thus obtained the title compound in equally good yield.

Sources & evidence

ORD record
ord-7b0a22d42e9d48fb9f5c637404085174
Source dataset
uspto-grants-1980_10
Patent number
US04230705

Reaction notes

Loading…