Acetohydrazide → HCID 23333675, compound

HRID 904126Notes

Reaction equation

[C:1]([CH:9]([CH3:15])[CH:10]([CH3:14])C(O)=O)(=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.C([NH:19][NH2:20])(=O)C.C(C(C)CC(O)=O)(=O)C1C=CC=CC=1.[C:35]([NH:39][NH2:40])(=O)[CH2:36][CH3:37]>>[CH2:36]([C:35]1[N:19]2[N:20]=[C:1]([C:2]3[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=3)[C:9]([CH3:15])=[CH:10][C:14]2=[N:40][N:39]=1)[CH3:37]

Participants

Reactant 4

HCID 14039Acetohydrazide

HCID 79890Propionylhydrazine

HCID 12240573HCID 12240573, compound

HCID 125590873-Benzoylbutyric acid

Product 1

HCID 23333675HCID 23333675, compound

Procedure

The general procedure of Example 4 is repeated but replacing the 3-benzoyl-2,3-dimethyl-propionic acid and N-acetylhydrazine employed in that example with 3-benzoyl-3-methyl-propionic acid and N-propionylhydrazine.

Sources & evidence

ORD record: ord-3aef79a2a430466eb26681fa10b24b7d
Source dataset: uspto-grants-1980_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04230705

Reaction notes

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