HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Bicarbonate → N-n-propyl-N-(2-ethoxycarbonylbenzyl)-4-ethoxycarbonylmethylaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | Ethyl 2-(bromomethyl)benzoate | HCID 11032082 | — |
| Reactant | N-n-propyl-4-ethoxycarbonylmethylaniline | HCID 23333610 | — |
| Solvent | Water | HCID 962 | — |
| Product | N-n-propyl-N-(2-ethoxycarbonylbenzyl)-4-ethoxycarbonylmethylaniline | HCID 23333601 | 85.8% |
Reaction Steps
N-n-propyl-4-ethoxycarbonylmethylaniline (11.1 g, b.p. 131°-135°C./0.5 mmHg), sodium hydrogencarbonate (6.3 g), water (10 ml), and ethyl 2-bromomethylbenzoate (14.6 g) were treated in the same manner as described in Example 1 to obtain N-n-propyl-N-(2-ethoxycarbonylbenzyl)-4-ethoxycarbonylmethylaniline (16.5 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04230703 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-f2fe747f834641ae9a57cc1fc66d20f3 |
| Source note | uspto-grants-1980_10 |