HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Bromomethyl)benzonitrile → HCID 23333579, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Bromomethyl)benzonitrile | HCID 89599 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | N-methyl-4-ethoxycarbonylmethylaniline | HCID 11550151 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 23333579 | HCID 23333579 | 112.8% |
Reaction Steps
N-Methyl-4-ethoxycarbonylmethylaniline (10 g), sodium hydrogencarbonate (5 g), water (5 ml), and 2-bromomethylcyanobenzene (12.2 g) were treated in the same manner as described in Example 1 for the preparation of the starting material. 18 g of N-methyl-N-(2-cyanobenzyl)-4-ethoxycarbonylmethylaniline was obtained as a light-yellow oily material.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04230703 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-c1ee446f2a1c4e14988399d4bded4515 |
| Source note | uspto-grants-1980_10 |