HCID 13015020, compound → HCID 23333629, compound

HRID 904192Notes

Reaction equation

HRID 904192 reaction equation
[CH3:1][N:2]1[CH2:8][C:7]2[CH:9]=[CH:10][CH:11]=[CH:12][C:6]=2[C:5](=[O:13])[C:4]2[CH:14]=[CH:15][C:16]([CH2:18][C:19]([OH:21])=[O:20])=[CH:17][C:3]1=2.[CH3:22]O.S(=O)(=O)(O)O>>[CH3:1][N:2]1[CH2:8][C:7]2[CH:9]=[CH:10][CH:11]=[CH:12][C:6]=2[C:5](=[O:13])[C:4]2[CH:14]=[CH:15][C:16]([CH2:18][C:19]([O:21][CH3:22])=[O:20])=[CH:17][C:3]1=2

Participants

3

Reactant 2

HCID 13015020HCID 13015020, compoundHCID 18363649Sulfuric acid methanol

Product 1

HCID 23333629HCID 23333629, compound

Procedure

5,6-Dihydro-5-methyl-11-oxodibenz[b,e]azepine-3-acetic acid was esterified with methanol-sulfuric acid in a customary manner to afford methyl 5,6-dihydro-5-methyl-11-oxodibenz[b,e]azepine-3-acetate having a melting point of 88.4°-90.5° C.

Sources & evidence

ORD record
ord-9c23df2de1d04ba88c2b461ff514e65a
Source dataset
uspto-grants-1980_10
Patent number
US04230703

Reaction notes

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