HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromomethylcyclopropane → HCID 70586749, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromomethylcyclopropane | HCID 81503 | — |
| Reactant | (Bromomethyl)cyclobutane | HCID 2734658 | — |
| Reactant | HCID 70586442 | HCID 70586442 | — |
| Product | HCID 70586749 | HCID 70586749 | 34% |
Reaction Steps
A sample of 3-methoxy-8β-methylmorphinan-6-one hydrochloride (prepared in Example 1C) was treated as in Example 1D, except that cyclobutylmethyl bromide (1.5 eq) was substituted for the cyclopropylmethyl bromide. The product was isolated as in Example 1D and converted to the hydrochloride salt, yield 34%, mp 217°-220° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04230712 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-b7ef6a0b18914503b8a8fb885b22b6ee |
| Source note | uspto-grants-1980_10 |