HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyanogen Bromide → HCID 53912372, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyanogen Bromide | HCID 10476 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 13245269 | HCID 13245269 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 53912372 | HCID 53912372 | — |
Reaction Steps
An 8.4 g sample of 3-methoxy-17-methylmorphinan-6-one (prepared as in Part 6A) in 85 ml of chloroform containing 6.09 g of dry K2CO3 was reacted with 3.8 g of cyanogen bromide and the product isolated as described in Example 1B. The product was crystallized from ethanol; yield 6.96 g (80%), mp 211°-214° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04230712 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-ba2117d1abc64428b86ee55055028c2e |
| Source note | uspto-grants-1980_10 |