HCID 22226923, compound → HCID 23334046, compound

HRID 904296Notes

Reaction equation

HRID 904296 reaction equation
[CH3:1][C:2]1[CH:3]=[C:4]2[C:9](=[CH:10][CH:11]=1)[O:8][C:7](=[O:12])[C:6]([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)=[C:5]2[OH:19].[O:20]1[CH2:25][CH2:24][N:23]([CH:26](Cl)[CH3:27])[CH2:22][CH2:21]1>>[CH3:1][C:2]1[CH:3]=[C:4]2[C:9](=[CH:10][CH:11]=1)[O:8][C:7](=[O:12])[C:6]([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)=[C:5]2[O:19][CH2:27][CH2:26][N:23]1[CH2:24][CH2:25][O:20][CH2:21][CH2:22]1

Participants

3

Reactant 2

HCID 22226923HCID 22226923, compoundHCID 54705874HCID 54705874, compound

Product 1

HCID 23334046HCID 23334046, compoundYield 77%

Procedure

This compound is prepared as described in Example 8 from 19.4 g. (0.077 mol) of 6-methyl-4-hydroxy-3-phenyl-coumarin and 16.1 g. (0.1 mol) of 2-morpholino-2-chlorethane. Weight 21.7 g.; yield 77% (theoretical yield 28.2 g.). M.P. 96° C.

Workup

  1. customThis compound is prepared

Sources & evidence

ORD record
ord-de49130d435546d18322eae1266cf994
Source dataset
uspto-grants-1980_10
Patent number
US04230850

Reaction notes

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