HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Phenylcyclohexanone → 3,8-Diphenyl-4-hydroxy-5,6,7,8-tetrahydrocoumarin
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Phenylcyclohexanone | HCID 95592 | — |
| Reactant | Ethyl phenyl malonate | HCID 53937759 | — |
| Reactant | Dipropyl ether ethanol | HCID 86734129 | — |
| Solvent | Diphenyl Ether | HCID 7583 | — |
| Product | 3,8-Diphenyl-4-hydroxy-5,6,7,8-tetrahydrocoumarin | HCID 54721331 | — |
Reaction Steps
Prepared according to the method of Example 14, Stage A, by thermal condensation in diphenyl ether of 2-phenyl-cyclohexanone and ethyl phenyl malonate. M.P. 185° C. (Dipropyl ether/ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04230850 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-b3652377ac844c75b929876d1141febe |
| Source note | uspto-grants-1980_10 |