HCID 13034082, compound → HCID 23334080, compound

HRID 904325Notes

Reaction equation

HRID 904325 reaction equation
[C:1]1([C:7]2[C:8](=[O:18])[O:9][C:10]3[C:15]([C:16]=2[OH:17])=[CH:14][CH:13]=[CH:12][CH:11]=3)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[N:19]1([CH2:25][CH:26]([CH3:29])[CH2:27]Cl)[CH2:24][CH2:23][CH2:22][CH2:21][CH2:20]1>CCCCCC>[N:19]1([CH2:25][CH:26]([CH3:29])[CH2:27][O:17][C:16]2[C:15]3[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=3)[O:9][C:8](=[O:18])[C:7]=2[C:1]2[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=2)[CH2:24][CH2:23][CH2:22][CH2:21][CH2:20]1

Participants

4

Reactant 2

HCID 13034082HCID 13034082, compoundHCID 54688870Coumarin, 4-hydroxy-3-phenyl-

Product 1

HCID 23334080HCID 23334080, compoundYield 77.5%

Reagents, catalysts & solvents 1

HCID 8058HexaneSolvent

Procedure

Prepared from 3-phenyl-4-hydroxy-coumarin and 3-piperidino-2-methyl-1-chloropropane, according to the method of Example 8. A light yellow solid is obtained. M.P. 86°-87° C. (hexane). Yield 77.5%.

Workup

  1. customA light yellow solid is obtained

Sources & evidence

ORD record
ord-e56c40ada9fa4ec3b4086b9f1543b39e
Source dataset
uspto-grants-1980_10
Patent number
US04230850

Reaction notes

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