4-(3-Chloro-2-methylpropyl)morpholine → HCID 23334063, compound

HRID 904329Notes

Reaction equation

HRID 904329 reaction equation
[OH:1][C:2]1[C:11]2[C:6](=[C:7]([CH3:12])[CH:8]=[CH:9][CH:10]=2)[O:5][C:4](=[O:13])[C:3]=1[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1.[O:20]1[CH2:25][CH2:24][N:23]([CH2:26][CH:27]([CH3:30])[CH2:28]Cl)[CH2:22][CH2:21]1>>[O:20]1[CH2:25][CH2:24][N:23]([CH2:26][CH:27]([CH3:30])[CH2:28][O:1][C:2]2[C:11]3[C:6](=[C:7]([CH3:12])[CH:8]=[CH:9][CH:10]=3)[O:5][C:4](=[O:13])[C:3]=2[C:14]2[CH:15]=[CH:16][CH:17]=[CH:18][CH:19]=2)[CH2:22][CH2:21]1

Participants

3

Reactant 2

HCID 233340474-(3-Chloro-2-methylpropyl)morpholineHCID 54721334HCID 54721334, compound

Product 1

HCID 23334063HCID 23334063, compoundYield 65%

Procedure

Prepared according to the method of Example 8 from 4-hydroxy-8-methyl-3-phenyl-coumarin and 3-morpholino-2-methyl-1-chloropropane. An oil is obtained which cannot be crystallised. Yield 65%.

Workup

  1. customPrepared
  2. customAn oil is obtained which
  3. customcannot be crystallised

Sources & evidence

ORD record
ord-ddc2cba6273b46b5baae49d778c2fc90
Source dataset
uspto-grants-1980_10
Patent number
US04230850

Reaction notes

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