HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → Methyl 3,5-dinitrobenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 3,5-Dinitrobenzoic acid | HCID 7433 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Methyl 3,5-dinitrobenzoate | HCID 222067 | 96% |
Reaction Steps
Following Example 11 but replacing the 1-(H)-tetrazolylacetic acid with 3,5-dinitrobenzoic acid, 3.39 g (1.6 cmoles) and the ethanol with methanol, 0.64 ml (1.6 cmoles), the ester was obtained with a yield of 96% (2.17 g), m.p.=108° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04230849 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-5bd2f4b322e649ce8dc3d0977ee1a34d |
| Source note | uspto-grants-1980_10 |