Methyl Isocyanate → HCID 178485936, compound

HRID 904381Notes

Reaction equation

HRID 904381 reaction equation
[NH:1]1[CH:5]=[CH:4][C:3]([CH2:6][NH:7][CH2:8][CH2:9][NH2:10])=[N:2]1.[CH3:11][N:12]=[C:13]=[O:14]>>[CH3:11][NH:12][C:13]([NH:10][CH2:9][CH2:8][NH:7][CH2:6][C:3]1[CH:4]=[CH:5][NH:1][N:2]=1)=[O:14]

Participants

3

Reactant 2

HCID 12228Methyl IsocyanateHCID 178511340HCID 178511340, compound

Product 1

HCID 178485936HCID 178485936, compound

Procedure

N-(3-Pyrazolylmethyl)ethylenediamine is reacted with methyl isocyanate by the procedure of Example 24 to give, after concentrating and separating the residue by colum chromatography, the title compound.

Workup

  1. customto give
  2. concentrationafter concentrating
  3. customseparating the residue by colum chromatography

Sources & evidence

ORD record
ord-93e9b093716346998052e5f824aa7b7d
Source dataset
uspto-grants-1980_10
Patent number
US04230865

Reaction notes

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