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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 904498Erstellt: 25. Oktober 2026

Chloroform → 3-[4-(4-Pentadecenylamino)benzoyl]-4-carboethoxythiazolidine

https://huagongshe.com/reaction/904498

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktChloroformHCID 6212—
EduktTriethylamineHCID 8471—
EduktEthyl thiazolidine-4-carboxylateHCID 103574—
EduktHCID 74042329HCID 74042329—
LösungsmittelDichloromethaneHCID 6344—
Produkt3-[4-(4-Pentadecenylamino)benzoyl]-4-carboethoxythiazolidineHCID 53653028—

Reaktionsschritte

One-tenth mole of 4-(4-pentadecenylamino)benzoyl chloride hydrochloride in methylene chloride is added to a solution of 0.1 mole of ethyl thiazolidine-4-carboxylate in chloroform containing two equivalents of triethylamine. After 5 hours at 20° C. the solution is filtered and evaporated to a white solid which is recrystallized from acetonitrile.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04230878
Quelldatensatzuspto-grants-1980_10
ORD IDord-e5dc31ffea4745cc8bbb28d2fb22a12b
Quellennotizuspto-grants-1980_10