HRID904619

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID10965249

Amino 4-methylbenzenesulfonate

C7H9NO3S

HCID14155664

未命名化合物

PRODUCTS

生成物

结构：Cc1ccc(S(=O)(=O)[O-])cc1.N[n+]1cc2ccccc2cc1C(=O)c1ccc(Cl)cc1

HCID14155665

未命名化合物

收率 73%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

5 g (19 millimoles) of 3-(4-chlorobenzoyl)-isoquinoline are dissolved in 10 ml of dichloromethane, then 4 g (22 millimoles) of O-(p-toluenesulfonyl)-hydroxylamine are added, and the mixture is allowed to stand for an hour. 6 g (73%) of 2-amino-3-(4-chlorobenzoyl)-isoquinolinium-p-toluene sulfonate are obtained.

WORKUP

后处理

waitto stand for an hour