HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 70534319, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 88738128 | HCID 88738128 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 70534319 | HCID 70534319 | 80% |
Reaction Steps
6.0 g (0.024 moles) of 1-oxo-pyrido[2,1-f]-as-triazinium perchlorate are boiled in acetonitrile in the presence of 6 ml of methyl iodide and 3.4 ml of triethylamine for an hour. 5.6 g of desired compound are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04419355 |
| Source dataset | uspto-grants-1983_12 |
| ORD ID | ord-131ffb8dc1434e0bbe70a64e1a6ea0cb |
| Source note | uspto-grants-1983_12 |