HuagongsheHuagongshe Chemistry Print Report · For research reference only
9-(2-cyclohexenyl)-2-propoxy-9H-adenine → 9-Cyclohexyl-2-n-propoxy-9H-adenine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 9-(2-cyclohexenyl)-2-propoxy-9H-adenine | HCID 12777830 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 9-Cyclohexyl-2-n-propoxy-9H-adenine | HCID 51814 | — |
Reaction Steps
A solution of 2.21 g (7.8 mmoles) of 9-(2-cyclohexenyl)-2-propoxy-9H-adenine in 30 mL of 90% ethanol was hydrogenated overnight with 250 mg of 10% palladium on carbon and then filtered. The filtrate was evaporated in vacuo, giving a residue which was crystallized from ethyl acetate--n-hexane. Yield 1.85 g (76%); melting point 148°-150° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04419358 |
| Source dataset | uspto-grants-1983_12 |
| ORD ID | ord-c2d9738041144ff48bc99cb88811306a |
| Source note | uspto-grants-1983_12 |