Ethanol → HCID 135838360, compound

Participants

Reaction Steps

The product of step (b) (6.5 g) was dissolved in dry ethanol (500 mls). Dry hydrogen chloride gas was then bubbled into this solution until a saturated solution resulted. This solution was heated on a steam bath for 1.5 hours. The mixture was poured into water and extracted into ether. The ethereal layer was washed with water, saturated sodium bicarbonate solution, dried using magnesium sulphate and filtered. On partial removal of the solvent a yellow solid crystallised out of solution. This was filtered off affording (1.1 g) of the sub-title compound. M.P. 150°-151° C.

Provenance & Evidence