HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 13543995, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 86739139 | HCID 86739139 | — |
| Product | HCID 13543995 | HCID 13543995 | — |
Reaction Steps
Ethyl 6-ethylthio-4-oxo-10-propyl-4H-pyrano[3,2-g]quinoline 2,8-dicarboxylate (2.85 g) was dissolved in ethanol (200 ml), and ethanol washed Raney nickel (30 g wet) added carefully. The mixture was refluxed for 11/2 hours, filtered to remove the catalyst, and concentrated, to give on cooling the title compound, (1.76 g) mp 168°-171° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04419352 |
| Source dataset | uspto-grants-1983_12 |
| ORD ID | ord-a58e0921b86842b5a443a25baf3c5106 |
| Source note | uspto-grants-1983_12 |