HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetylacetone → HCID 20477992, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetylacetone | HCID 31261 | — |
| Reactant | HCID 178472135 | HCID 178472135 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 20477992 | HCID 20477992 | — |
Reaction Steps
A solution of crude ethyl 3-(2-dimethylamino-ethylamino)-3-iminopropionate (15.3 g, 50 mmol) and pentane-2,4-dione (7.7 ml, 75 mmol) in dry benzene (80 ml) is refluxed for 18 hours. This solution is dried over anhydrous sodium sulfate and evaporated to give 18.4 g of crude title B product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04420615 |
| Source dataset | uspto-grants-1983_12 |
| ORD ID | ord-4fbc5dbf45304335bf51b2ebe39082c3 |
| Source note | uspto-grants-1983_12 |