HRID904925

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID7360

Tetrahydrofurfuryl alcohol

C5H10O2

HCID175460

2-[4-(3-Methylbut-2-en-1-yl)phenyl]propanoic acid

C14H18O2

PRODUCTS

生成物

HCID13118087

未命名化合物

收率 81.1%

AUXILIARIES

试剂、催化剂与溶剂

结构：C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.C.O=S(=O)(O)O.O=S(=O)(O)O.O=S(=O)(O)O.O=S(=O)(O)O.O=S(=O)(O)O.O=S(=O)(O)O.O=S(=O)(O)O

催化剂HCID73357732

未命名化合物

溶剂HCID8078

Cyclohexane

C6H12

PROCEDURE

实验过程

A mixture of 21.8 g of 2-(p-prenylphenyl)propionic acid, 10.2 g of tetrahydrofurfuryl alcohol and 0.4 g of graphite bisulfate in 100 ml of cyclohexane was stirred at room temperature for 8 hours. The mixture was passed through a column of silica gel, and the solvent was evaporated to give 24.5 g of tetrahydrofurfuryl 2-(p-prenylphenyl)propionate. b.p. 135° C./0.08 mmHg, IR νmaxneat ; 1730 cm-1.

WORKUP

后处理

customthe solvent was evaporated