HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyl Formate → Dibutyl Oxalate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyl Formate | HCID 11614 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | Dibutyl Oxalate | HCID 16306 | — |
Reaction Steps
Experiment was run in the same manner as in Example 4 except that the catalyst was replaced by 1.0 wt.% palladium-on-silicon-carbide. As the result, it was found that n-butyl formate was produced in a space time yield of 202 g./l.-catalyst.hr and small amounts of di-n-butyl oxalate and n-butanol were by-produced.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04420633 |
| Source dataset | uspto-grants-1983_12 |
| ORD ID | ord-57f0fcd15f7c4a6a815b1edb34f42b7d |
| Source note | uspto-grants-1983_12 |