HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diazomethane → HCID 54197768, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | 2-Propenoic acid, 3-bromo-2,3-diiodo- | HCID 53705266 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 54197768 | HCID 54197768 | — |
Reaction Steps
0.5 g of 3-bromo-2,3-diiodoacrylic acid was dissolved in 20 ml of diethyl ether. A solution of diazomethane in diethyl ether was then added until nitrogen gas was no longer produced, whereupon the mixture was left to stand for 15 minutes. The diethyl ether was distilled off, giving 0.50 g of the desired compound as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04421766 |
| Source dataset | uspto-grants-1983_12 |
| ORD ID | ord-3eba91ebb1b445488da230ad2c3e577a |
| Source note | uspto-grants-1983_12 |