HuagongsheHuagongshe Chemistry Print Report · For research reference only
Imidazole → HCID 13079736, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Imidazole | HCID 795 | — |
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | HCID 54561442 | HCID 54561442 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 13079736 | HCID 13079736 | — |
Reaction Steps
130 mg of the isomer of lesser polarity of trans-6-(4-chlorobenzylthiomethyl)-2-[2-bromo-1-(2,4-dichlorophenyl)ethoxy]tetrahydropyran, 67.5 mg of imidazole and 74 mg of sodium iodide were reacted in dimethylformamide at 130° C. for 9 hours and then treated and the product purified essentially as described in Example 34(b)(i), to give 60 mg of the title compound in the form of a colourless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04421758 |
| Source dataset | uspto-grants-1983_12 |
| ORD ID | ord-028f32322ed44a558c60e2dad351637f |
| Source note | uspto-grants-1983_12 |