HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → Trimethylhydroquinone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Selenium Dioxide | HCID 24007 | — |
| Reactant | Benzenamine, 4,4'-(phenylmethylene)bis[N,N-diethyl-3-methyl- | HCID 84752 | — |
| Product | Trimethylhydroquinone | HCID 12785 | 234.9% |
Reaction Steps
After dissolving 45 mg of selenium dioxide, 0.4 g of a polycarbonate resin (having the same composition as the resin used for CTL in Example 1), and 280 mg of 4,4'-benzylidenebis(N,N-diethyl-m-toluidine) in 5 g of N,N-dimethylformamide and then dissolving therein 145 mg of trimethylhydroquinone, the solution obtained was immediately coated on an aluminum-vapor deposited polyester film (same as in Example 1) using a coating rod and dried for one hour under hot blast of 60° C. to form a photoconductive layer. The color of the photoconductive layer was deep red and the thickness was 8 μm. The photoconductive layer was heat-treated as in Example 1. The initial light discharge speed was 0.7 (V0 =-350 volts (saturated potential)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04421838 |
| Source dataset | uspto-grants-1983_12 |
| ORD ID | ord-d65f2b3888d54d768196e1f22f595cbf |
| Source note | uspto-grants-1983_12 |