HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 54349136, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 73679344 | HCID 73679344 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 54349136 | HCID 54349136 | — |
Reaction Steps
9.6 g of the ester obtained in step (a) are dissolved in 150 ml of ether and 20 ml of 5 N hydrochloric acid are added. Stirring is carried out for 12 hours. After extraction by the (1:1) v/v ether-CH2Cl2 mixture, then washings with water, 7.5 g of the expected product are obtained after evaporation of the organic phases. m.p.=90° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04421927 |
| Source dataset | uspto-grants-1983_12 |
| ORD ID | ord-c798cf13b745432ab6208e6f054fd393 |
| Source note | uspto-grants-1983_12 |