HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Toluenesulfonyl chloride → (2-Methyl-4,5,6,7-tetrahydro-1,3-benzothiazol-5-yl)methyl 4-methylbenzene-1-sulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Toluenesulfonyl chloride | HCID 7397 | — |
| Reactant | (2-Methyl-4,5,6,7-tetrahydro-1,3-benzothiazol-5-yl)methanol | HCID 3018726 | — |
| Product | (2-Methyl-4,5,6,7-tetrahydro-1,3-benzothiazol-5-yl)methyl 4-methylbenzene-1-sulfonate | HCID 3018727 | 74% |
Reaction Steps
The compound is prepared by action of p-toluenesulfonyl chloride on the above alcohol (IV), according to the procedure described in Example 1. M.p.=105°-106° C. Yield: 74%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04423056 |
| Source dataset | uspto-grants-1983_12 |
| ORD ID | ord-ac197eb5f6f84fe88ca531e9a5ff0721 |
| Source note | uspto-grants-1983_12 |