Ammonia → HCID 3059961, compound

HRID 905192Notes

Reaction equation

HRID 905192 reaction equation
[NH3:1].S(O[CH2:13][CH:14]1[CH2:22][CH2:21][C:17]2[N:18]=[CH:19][S:20][C:16]=2[CH2:15]1)(C1C=CC(C)=CC=1)(=O)=O>CO>[NH2:1][CH2:13][CH:14]1[CH2:22][CH2:21][C:17]2[N:18]=[CH:19][S:20][C:16]=2[CH2:15]1

Participants

4

Reactant 2

HCID 222AmmoniaHCID 12917759HCID 12917759, compound

Product 1

HCID 3059961HCID 3059961, compoundYield 42%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The compound is prepared by action of ammonia on the above tosylate (V), in methanol, in a autoclave at 100° C. B.p.0.5 =100°-106° C. Yield: 42%.

Workup

  1. customB.p.0.5 =100°-106° C

Sources & evidence

ORD record
ord-f07224cce4c44b84b7ab6722033b38cb
Source dataset
uspto-grants-1983_12
Patent number
US04423056

Reaction notes

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