Diethyl Ether → HCID 12917753, compound

HRID 905193Notes

Reaction equation

HRID 905193 reaction equation

C(O[C:4]([CH:6]1[CH2:14][CH2:13][C:9]2[N:10]=[CH:11][S:12][C:8]=2[CH2:7]1)=[O:5])C.[CH3:15][CH2:16]OCC>>[CH2:15]([C:11]1[S:12][C:8]2[CH2:7][CH:6]([CH2:4][OH:5])[CH2:14][CH2:13][C:9]=2[N:10]=1)[CH3:16]

Participants

3

Reactant 2

HCID 3283Diethyl Ether

HCID 12917744HCID 12917744, compound

Product 1

HCID 12917753HCID 12917753, compoundYield 86%

Procedure

The compound is prepared by reduction of the above derivative (III) with AlLiH4 within ether, at room temperature. B.p.0.5 =142°-144° C. Yield: 86%.

Workup

customB.p.0.5 =142°-144° C

Sources & evidence

ORD record: ord-0e24bb7c1c1c459b8b267e0d28d6ef2f
Source dataset: uspto-grants-1983_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04423056

Reaction notes

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