HCID 12917741, compound → HCID 12917754, compound

HRID 905195Notes

Reaction equation

HRID 905195 reaction equation
[CH2:1]([C:5]1[S:6][C:7]2[CH2:13][CH2:12][CH2:11][CH:10]([C:14](OCC)=[O:15])[C:8]=2[N:9]=1)[CH2:2][CH2:3][CH3:4]>CCOCC>[CH2:1]([C:5]1[S:6][C:7]2[CH2:13][CH2:12][CH2:11][CH:10]([CH2:14][OH:15])[C:8]=2[N:9]=1)[CH2:2][CH2:3][CH3:4]

Participants

3

Reactant 1

HCID 12917741HCID 12917741, compound

Product 1

HCID 12917754HCID 12917754, compoundYield 48%

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

The compound is prepared by reduction of the above derivative (III), with AlLiH4 in ether at room temperature. B.p.0.6 =130°-132° C. Yield:48%.

Workup

  1. customB.p.0.6 =130°-132° C

Sources & evidence

ORD record
ord-2a155afb6eb942e8aca84535ab6bb982
Source dataset
uspto-grants-1983_12
Patent number
US04423056

Reaction notes

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