HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12917743, compound → 2-n-Butyl-5-hydroxymethyl-4,5,6,7-tetrahydrobenzo[d]thiazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12917743 | HCID 12917743 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 2-n-Butyl-5-hydroxymethyl-4,5,6,7-tetrahydrobenzo[d]thiazole | HCID 12917755 | 89% |
Reaction Steps
The compound is prepared by reduction of the above derivative (III) with AlLiH4 in ether at room temperature. B.p.0.15 =138°-142° C. Yield: 89%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04423056 |
| Source dataset | uspto-grants-1983_12 |
| ORD ID | ord-a42dbfeb98254686b54a22a383fc4077 |
| Source note | uspto-grants-1983_12 |