HCID 12917742, compound → HCID 12917756, compound

HRID 905199Notes

Reaction equation

HRID 905199 reaction equation
[CH:1]([C:4]1[S:5][C:6]2[CH2:12][CH2:11][CH:10]([C:13](OCC)=[O:14])[CH2:9][C:7]=2[N:8]=1)([CH3:3])[CH3:2]>CCOCC>[CH:1]([C:4]1[S:5][C:6]2[CH2:12][CH2:11][CH:10]([CH2:13][OH:14])[CH2:9][C:7]=2[N:8]=1)([CH3:3])[CH3:2]

Participants

3

Reactant 1

HCID 12917742HCID 12917742, compound

Product 1

HCID 12917756HCID 12917756, compoundYield 83%

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

The compound is prepared by reduction of the above derivative (III) with AlLiH4 in ether at room temperature. B.p.0.1 =122°-126° C. Yield: 83%.

Workup

  1. customB.p.0.1 =122°-126° C

Sources & evidence

ORD record
ord-4970b355f6c542169f62978ec0e2a6b1
Source dataset
uspto-grants-1983_12
Patent number
US04423056

Reaction notes

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