Triethylamine → HCID 54285389, compound

Participants

Reaction Steps

A mixture of 5-chloropyrimidine-2-thione (4.3 mmol), 2,3,5-tri-O-benzoyl-β-D-ribofuranosyl chloride (4.3 mmol) and triethylamine (4.3 mmol) in dichloromethane (25 ml) was stirred together at room temperature for 4 h, the mixture evaporated and the residue triturated with water; the residue was the title compound; yield 28% 1H NMR (CDCl3): δ4.75 (CH2), 6.0-6.5 (4 H), 7.2-8.2 (3 Ph), 8.50 (H-4, H-6).

Provenance & Evidence