Diethanolamine → HCID 20476169, compound

Participants

Reaction Steps

Into a perfectly clean and dry flask were introduced 105.1 g (1 mol) of rectified diethanolamine and 1600 ml of anhydrous pyridine. While stirring, 507.4 g (3.12 mols) of di-n-propylacetyl chloride were added in 30 to 45 minutes, care being taken to maintain the temperature below +30° C. The reaction medium was then stirred at room-temperature for 48 hours.

Provenance & Evidence