HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxybenzoic acid → 65046-95-9
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxybenzoic acid | HCID 11370 | — |
| Reactant | Zinc Oxide | HCID 3007857 | — |
| Solvent | Water | HCID 962 | — |
| Product | 65046-95-9 | HCID 70359634 | 70% |
Reaction Steps
Zinc o-methoxybenzoate was prepared by mixing 32.6 g of zinc oxide with 138 g of o-methoxybenzoic acid and 600 g of water and refluxing for 4 hours. After cooling in an ice bath, the solid was filtered off and dried in a vacuum oven at 25 mm Hg and 50° C. to yield 103 g of zinc o-methoxybenzoate. An elemental analysis gave 52.8% C, 3.95% H and 16.0% Zn (calculated: 52.26% C, 3.81% H and 17.8% Zn).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04423182 |
| Source dataset | uspto-grants-1983_12 |
| ORD ID | ord-8a595024159b4cc7bff7ef3088c33829 |
| Source note | uspto-grants-1983_12 |