HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon Dioxide → HCID 131729141, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon Dioxide | HCID 280 | — |
| Reactant | 2,2,3,3-Tetrafluorobutanedioic acid | HCID 67833 | — |
| Reactant | Carbonic acid-guanidine (1:1) | HCID 286947 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 131729141 | HCID 131729141 | — |
Reaction Steps
Tetrafluorosuccinic acid (500 mg, 2.63 mmol) was dissolved in 10 ml of distilled water. Guanidine carbonate (474 mg, 2.63 mmol) was added at room temperature (carbon dioxide gas was evolved) and the reaction was stirred at room temperature for 2 hours. The water was removed in vacuo with heating to approximately 90° C. for 4 hours. The product was isolated as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08012277B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-4824c440447a4d9ba0f412b5f293d0b2 |
| Source note | uspto-grants-2011_09 |