Carbon Dioxide → HCID 178514407, compound

HRID 905507Notes

Reaction equation

HRID 905507 reaction equation
[C:1]([OH:6])(=[O:5])[C:2]([OH:4])=[O:3].C(=O)(O)O.[NH2:11][NH:12][C:13]([NH2:15])=[NH:14].C(=O)=O>O>[C:1]([O-:6])(=[O:5])[C:2]([O-:4])=[O:3].[NH2:11][NH:12][C:13]([NH2:15])=[NH2+:14].[NH2:11][NH:12][C:13]([NH2:15])=[NH2+:14]

Participants

5

Reactant 3

HCID 280Carbon DioxideHCID 971Oxalic AcidHCID 178513185HCID 178513185, compound

Product 1

HCID 178514407HCID 178514407, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Oxalic acid (2.00 g, 22.20 mmol) was dissolved in 40 ml of distilled water. Aminoguanidine bicarbonate (6.05 g, 44.40 mmol) was added via syringe at room temperature (carbon dioxide gas was evolved) and the reaction was stirred at room temperature for 24 hours. The water was removed in vacuo with heating to approximately 90° C. for 4 hours. The product was isolated as a white solid.

Workup

  1. customThe water was removed in vacuo
  2. temperaturewith heating to approximately 90° C. for 4 hours
  3. customThe product was isolated as a white solid

Sources & evidence

ORD record
ord-2f6f5fc3b2254932b231af1cf08beff1
Source dataset
uspto-grants-2011_09
Patent number
US08012277B2

Reaction notes

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