Carbon Dioxide → HCID 178514409, compound

HRID 905514Notes

Reaction equation

HRID 905514 reaction equation
[C:1]([OH:9])(=[O:8])/[C:2](=[C:4](\[CH:6]=[O:7])/[Br:5])/[Br:3].C(=O)(O)O.[NH2:14][NH:15][C:16]([NH2:18])=[NH:17].C(=O)=O>O>[C:1]([O-:9])(=[O:8])/[C:2](=[C:4](\[CH:6]=[O:7])/[Br:5])/[Br:3].[NH2:14][NH:15][C:16]([NH2:18])=[NH2+:17]

Participants

5

Reactant 3

HCID 280Carbon DioxideHCID 3033972Mucobromic AcidHCID 178513185HCID 178513185, compound

Product 1

HCID 178514409HCID 178514409, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Mucobromic acid (2.0 g, 7.76 mmol) was dissolved in 10 ml of distilled water. Aminoguanidine bicarbonate (1.06 g, 7.76 mmol) was added in portions at room temperature (carbon dioxide gas was evolved) and the reaction was stirred at room temperature for 18 hours. The water was removed in vacuo with heating to approximately 90° C. The product was isolated as an off-white solid.

Workup

  1. customThe water was removed in vacuo
  2. temperaturewith heating to approximately 90° C
  3. customThe product was isolated as an off-white solid

Sources & evidence

ORD record
ord-4f35ba68c5da457ab8339458b719f25e
Source dataset
uspto-grants-2011_09
Patent number
US08012277B2

Reaction notes

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