Benzylamine → HCID 67385729, compound
Reaction equation
[C:1]([N:4]1[CH2:10][CH2:9][CH:8]([CH3:11])[C:7](=O)[CH2:6][CH2:5]1)(=[O:3])[CH3:2].[CH2:13]([NH2:20])[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1>>[CH2:13]([NH:20][CH:7]1[CH:8]([CH3:11])[CH2:9][CH2:10][N:4]([C:1](=[O:3])[CH3:2])[CH2:5][CH2:6]1)[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1Participants
3
Procedure
Racemic 1-(4-benzylamino-5-methyl-azepan-1-yl)-ethanone was prepared in the same manner from racemic 1-acetyl-5-methyl-azepan-4-one. In this instance, benzylamine was used instead of (R)-1-phenylethylamine.
Sources & evidence
- ORD record
- ord-d79541262c504529a98d754093903db1
- Source dataset
- uspto-grants-2011_09
- Patent number
- US08012974B2
Reaction notes
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