Methyl chloroformate → Methyl 3-methyl-4-oxopiperidine-1-carboxylate

HRID 905966Notizen

Reaktionsgleichung

Cl.[CH3:2][CH:3]1[C:8](=[O:9])[CH2:7][CH2:6][NH:5][CH2:4]1.Cl[C:11]([O:13][CH3:14])=[O:12]>>[CH3:14][O:13][C:11]([N:5]1[CH2:6][CH2:7][C:8](=[O:9])[CH:3]([CH3:2])[CH2:4]1)=[O:12]

Komponenten

Edukt 2

HCID 6586Methyl chloroformate

HCID 227288643-Methyl-piperidin-4-one hydrochloride

Produkt 1

HCID 3015586Methyl 3-methyl-4-oxopiperidine-1-carboxylate

Versuchsvorschrift

Racemic 3-methyl-4-oxo-piperidine-1-carboxylic acid methyl ester was prepared in the same manner from racemic 3-methyl-piperidin-4-one hydrochloride and methyl chloroformate.

Quellen und Nachweise

ORD-Eintrag: ord-61dcdcdc0bd84f4393dbfb72489eba1a
Quelldatensatz: uspto-grants-2011_09
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US08012974B2

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